Page 183 - 006
P. 183
177
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1) M U %:# (gas supply)
!' % V! & 6/ '*
! 8 "
/
6/
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,
6
,
("
* %5 * U "
& # 5(
5 (
6
% (
,
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+7
6/
)
6/
7
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#% ( & * ( (detector) V! & 6/ ' * H)
! &
! &
1
V 3 ' & #&0
5 .6/
4
5 & ' /
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)
6/
2) " O $ (injector) ! '! " * H)
8( ! & "
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5
'* !& (column) . '
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&,
# K 0 - ' !
)
,
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/
1
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)
injector & 0 - '! . '* ' ! " ! H "5( 5 '
1
1
0
6
)
! ! " ! 2* !
*( ( ( ! 50 °C " injector 5(
split, splitless, on column
,
1
/
0
3) ; (column) & !
#'! & 2'!(
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!
/
R
,
^
,
Y
("' / 5 & ! #
! &
V 2 -'&6 .&& (pack column)
1
+
Y
& c & , (capillary column) ( ) ' / 10.7) .&& ,* solid support "(
,
/
V!& ' & " 1.5-10 ! 3 $) "
- " 2-4 ' /
& c & , ! 3 $) ",
- " "
( # H+ 10 ' ! H #
+/
5( 2 % ( &6 wall-coated open tubular (WCOT) 3 - " H)
& 6 #5 ( " V!
& '' support-coated open tubular (SCOT) 3 - " H)
& 6 #5
/
+/
/
6/
( "! % # K . (( # V!& ' ("' 5 SCOT * !'L - . "
7
/
/
)
WCOT " 5
Y ' 7 &)
Y ! 'L - .' /(
.Y&& ,
A
B
$X 10.7 % ( & , A: pack column, B: capillary column (Department of
Chemistry 2007, Advanced Technology and Industrial Co. Ltd., 2007)
7
,
0
4) 8 $ "$ U O (detector) & * ( 0
% !(' "
!
6/
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V ' '
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%
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0
5 " ## 3 **# * % ##
& #&0 3 ' & . *
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67
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)
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4 8.
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5 ' 10.3 !(
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1
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4 8. & 6/ * (% ( K ' / % & 6/ 6
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V